We offer a full range of X-ray diffraction (XRD) testing services for powders, single crystals, thin films, and nanomaterials. Our expertise covers phase identification, lattice parameter measurement, high-resolution thin-film analysis, nanoscale structure characterization, and in-situ monitoring of structural changes. Using advanced instruments and optimized testing protocols, we provide accurate, reproducible, and high-quality data for research, development, and industrial applications. Customers rely on our experience for precise structural insights, quick turnaround, and professional support, making us a trusted partner in material characterization. Our services help drive innovation and ensure quality across scientific and industrial fields.
X-ray diffraction is a technique used to analyze the crystalline structure, phase composition, and properties of solid materials. It is commonly applied to powders, thin films, metals, minerals, and other crystalline samples in materials science, chemistry, and engineering. XRD works by directing X-rays onto a crystal lattice, where the rays are diffracted according to Bragg's Law:
nλ=2dsinθ
Here, n is the reflection order, λ is the X-ray wavelength, d is the spacing between lattice planes, and θ is the incidence angle. The resulting diffraction pattern is unique to the material, allowing identification and determination of lattice parameters.
Suitable for powders, bulk, or polycrystalline samples, providing phase identification, quantitative analysis, and lattice parameter determination. Measurements are optimized for accuracy and reproducibility, supporting material characterization and quality control.
Single-crystal XRD enables detailed analysis of complete crystals, delivering atomic coordinates, bond lengths, and bond angles. This service supports molecular structure confirmation, precise crystallographic studies, and accurate characterization of complex single-crystal materials.
Micro-area XRD allows diffraction measurements on small localized regions, typically 5 × 5 mm or larger. This technique rapidly acquires high-quality diffraction patterns from heterogeneous or limited sample areas, supporting focused structural analysis.
Wide-angle XRD measures diffraction across ~5°–90°, providing comprehensive phase analysis and lattice parameter determination. This approach is widely used for bulk material characterization and crystallographic studies in both research and industrial applications.
Small-angle XRD (SAXS) detects scattering at low angles (0.5°–10°), revealing nanoscale structures, pore sizes, and particle distributions. It is ideal for nanomaterials characterization and studies of porous or self-assembled structures.
Variable-temperature XRD performs in-situ measurements between –40 ℃ and 1450 ℃, enabling the study of thermal effects, phase transitions, and structural stability, supporting materials research and high-temperature process investigations.
GIXRD is designed for thin-film and surface analysis using low incidence angles to emphasize diffraction from surface layers. This technique is ideal for studying thin films, coatings, interfaces, and surface crystallography.
High-resolution XRD uses precision optics and detectors to achieve narrow peak widths and high angular resolution. It is commonly applied to evaluate epitaxial thin films, microstructural quality, and subtle crystallographic features.
In-situ XRD continuously collects diffraction data during heating, cooling, pressure changes, or chemical reactions. It enables real-time observation of structural transformations, reaction kinetics, and dynamic phase transitions in various materials.
Contact us with your sample details, and we will recommend the XRD techniques best suited for your analysis needs.
Our XRD testing supports a wide range of samples, including powders, single crystals, bulk or polycrystalline solids, thin films and coatings, nanomaterials, and composites or mixtures. Each type is suitable for detailed phase, structural, and lattice analysis in research and industrial applications.
Samples must meet key criteria for accurate XRD analysis: powders and composites should be well-dispersed; single crystals intact; particle size and thickness appropriate; surfaces clean and free of contaminants; and all samples chemically and physically stable under testing conditions.
Samples requiring XRD testing, with or without prior preparation, can be submitted using our Sample Submission Form.
XRD analysis is widely applied for phase identification, lattice parameter measurement, and structural characterization. Materials science teams often face challenges such as complex multi-phase systems, nanoscale features, and high precision requirements. Our services deliver accurate diffraction data, supporting research, property validation, and innovative material development.
XRD testing is essential for crystal form identification, polymorph analysis, and solid-state characterization of APIs. Pharmaceutical developers often face challenges such as subtle polymorphic differences and limited in-house instrumentation. Our services deliver precise structural insights, supporting formulation optimization, stability studies, and reliable material characterization.
XRD techniques, including thin-film and high-resolution analysis, are widely used for semiconductor, coating, and device material characterization. Electronics companies face challenges such as epitaxial layer evaluation, crystallographic orientation control, and thin-film uniformity. Our testing solutions deliver reliable structural data, enabling product optimization and performance validation.
XRD is routinely applied for phase verification, crystallinity assessment, and production consistency monitoring. Quality control teams often face challenges such as batch-to-batch variability, complex material systems, and high reproducibility demands. Our services provide accurate, high-throughput analysis to ensure consistent product quality and support process optimization.
Our XRD services offer precise structural, phase, and lattice analysis for research, development, and quality control. Collaborate with our specialists to create a customized testing plan that enhances material understanding, supports innovation, and ensures project success.
Clients provide sample details and testing objectives via form, email, or phone. Our team evaluates requirements and recommends tailored XRD solutions.
Samples are securely sent to our laboratory. Upon arrival, each sample is logged, verified, and tracked to ensure integrity and traceability.
Our scientists develop a comprehensive XRD test plan, specifying measurement parameters, data collection methods, and analysis approach for accurate results.
The lab team conducts X-ray diffraction testing according to the plan, monitoring the process and optimizing parameters for reliable, reproducible data.
Collected data is processed with professional software. A structured report including diffraction patterns, phase analysis, and key conclusions is prepared.
The final report is delivered electronically or in print. Our experts provide interpretation and consultation to support research, production, or quality control.
We operate high-resolution powder and single-crystal XRD systems, capable of analyzing various sample sizes with exceptional sensitivity and reliability for precise structural characterization.
Our materials science and solid-state chemistry specialists deliver qualitative and semi-quantitative XRD analysis, offering actionable insights for complex crystalline systems.
Through partnerships with international laboratories, instrument vendors, and research institutions, we efficiently address challenging samples and provide tailored analytical solutions.
Reports integrate experiment design, data acquisition, diffraction analysis, and conclusions, ensuring consistency and actionable insights for material research and process optimization.
BOC Sciences' XRD Testing services support a wide range of applications, including but not limited to the following areas.
Client: A multinational specialty chemicals company
Challenge: The client required identification and comparison of polymorphic forms in crystalline intermediates to support formulation research and solid-state characterization.
Solution: BOC Sciences deployed high-precision XRD with automated phase identification and quantitative polymorph analysis. Our team conducted detailed diffraction pattern analysis and lattice parameter determination, providing clear differentiation between multiple polymorphic forms.
Outcome: The client obtained robust structural insights, facilitating rational selection of the optimal crystalline form. This streamlined material selection for R&D projects and minimized uncertainty in downstream processing.
Client: A leading materials research institute in Germany
Challenge: The client required precise identification of crystalline phases in newly developed high-performance ceramic materials, where overlapping diffraction peaks complicated phase differentiation.
Solution: BOC Sciences utilized high-resolution X-ray diffraction instruments combined with Rietveld refinement analysis. Our team optimized scan parameters, applied advanced peak deconvolution methods, and provided comprehensive phase mapping for multi-component ceramics.
Outcome: The client obtained accurate phase compositions, enabling informed materials optimization. This enhanced their product development workflow, reducing trial-and-error iterations and improving material performance predictability.
Client: A major Asian lithium-ion battery manufacturer
Challenge: The client needed a detailed crystallographic analysis of cathode powders to ensure consistent lattice structures and detect minor phase impurities that could affect electrochemical performance.
Solution: BOC Sciences applied powder XRD with quantitative phase analysis and texture measurements. Customized sample preparation and scanning protocols ensured reproducible diffraction patterns. Data interpretation included lattice parameter refinement and crystallite size analysis to evaluate structural integrity.
Outcome: The client achieved precise structural characterization, allowing early detection of potential defects. This contributed to improved battery efficiency and reliability, supporting high-performance product development.
The XRD testing service from BOC Sciences provided highly reliable phase identification for our complex material samples. Their detailed diffraction analysis and clear data presentation allowed our team to make informed decisions on material selection with confidence.
— Dr. M., Senior Materials Scientist, Advanced Materials Company
BOC Sciences' XRD testing offered comprehensive insights into the crystallographic structures of our compounds. The precision and clarity of their diffraction patterns enabled us to optimize our synthesis processes efficiently.
— Dr. S., R&D Manager, Specialty Chemicals Firm
The XRD analysis provided by BOC Sciences consistently produced accurate and reproducible results. Their meticulous attention to peak interpretation and pattern matching greatly enhanced our materials characterization workflows.
— Dr. T., Lead Researcher, Nanomaterials Startup
BOC Sciences' XRD service stands out for their expert data interpretation. Beyond delivering raw diffraction data, their team offered insightful analysis that significantly supported our material development strategies.
— Dr. R., Head of Materials Development, Industrial Coatings Company
